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#microstrain #originlab #sayphysics 00:10 strain calculation from XRD data 02:30 estimation of microstrain using origin 05:20 determine the microstrain using origin 07:45 XRD characterization of microstrain in origin 08:50 estimation of lattice strain from xrd in origin How to calculate microstrain from XRD data using origin Origin and Excel Files: https://drive.google.com/file/d/1dENsIopyAFHvHewBjctCy4L_K1OCyege/view?usp=sharing "X-ray diffraction analysis" "Microstrain calculation" "OriginLab software" "Data plotting" "Analyzing XRD data" "Materials characterization" "Crystallography" "Materials science" "Engineering" "Scientific data analysis" "Research methodology" "Experimental techniques" "Structural analysis" "Peak fitting" "Surface analysis" "Thin films" "Crystal defects" "Stress analysis" "Non-destructive testing" "X-ray spectroscopy" All XRD Video Tutorials: 1. Baseline correction for XRD and FTIR data https://youtu.be/0PUTB0IhlWw 2. How to smooth XRD graph https://youtu.be/asxWjB9MSiE 3. How to calculate the crystallite size from XRD data https://youtu.be/lZ1VESKBxKY 4. How to put negative hkl indices in XRD graph https://youtu.be/Jq4kRfrtJA8 5. How to plot and match XRD data in WinXPow https://youtu.be/r1EKRfV4ZRg 6. How to calculate crystallinity index from XRD data https://youtu.be/D65k1yHPKaM 7. How to calculate d-spacing (interplanar spacing) from XRD data https://youtu.be/0lz3ZMSdbAM 8. How to calculate lattice constants from XRD data https://youtu.be/0lz3ZMSdbAM 9. How to calculate microstrain from XRD data https://youtu.be/oUwJpGtwOVk 10. How to calculate dislocation density from XRD data https://youtu.be/WyvwytYYSK8 11. How to subtract instrumental broadening (Kα1 and Kα2 overlap) from XRD data https://youtu.be/238yM0OgaH8 12. How to subtract instrumental broadening (βi) from XRD data https://youtu.be/tO_frVLxmsg 13. Williamson-Hall Plot | W-H Plot | Crystallite Size | Microstrain | XRD data https://youtu.be/tO_frVLxmsg 14. Williamson-Hall Plot | W-H Plot | Crystallite Size | Microstrain | XRD data https://youtu.be/ipX3iUJ5VcU 15. Modified W-H Plots | UDM-USDM-UDEDM | Crystallite Size | Microstrain | Energy Density https://youtu.be/OG-G6V9X8l0 References: http://prism.mit.edu/xray Textbook References •HP Klug and LE Alexander, X-Ray Diffraction Procedures for Polycrystalline and Amorphous Materials, 2nd edition, John Wiley & Sons, 1974. https://www.wiley.com/en-us/X+Ray+Diffraction+Procedures%3A+For+Polycrystalline+and+Amorphous+Materials%2C+2nd+Edition-p-9780471493693 –Chapter 9: Crystallite Size and Lattice Strains from Line Broadening •BE Warren, X-Ray Diffraction, Addison-Wesley, 1969 –reprinted in 1990 by Dover Publications https://link.springer.com/article/10.1007/BF00482725 –Chapter 13: Diffraction by Imperfect Crystals •DL Bish and JE Post (eds), Reviews in Mineralogy vol 20: Modern Powder Diffraction, Mineralogical Society of America, 1989. –Chapter 6: Diffraction by Small and Disordered Crystals, by RC Reynolds, Jr. –Chapter 8: Profile Fitting of Powder Diffraction Patterns, by SA Howard and KD Preston •A. Guinier, X-Ray Diffraction in Crystals, Imperfect Crystals, and Amorphous Bodies, Dunod, 1956. –reprinted in 1994 by Dover Publications Article References https://link.springer.com/article/10.1007/s40094-014-0141-9 D. Balzar, N. Audebrand, M. Daymond, A. Fitch, A. Hewat, J.I. Langford, A. Le Bail, D. Louër, O. Masson, C.N. McCowan, N.C. Popa, P.W. Stephens, B. Toby, “Size-Strain Line-Broadening Analysis of the Ceria Round-Robin Sample”, Journal of Applied Crystallography 37 (2004) 911-924 •S Enzo, G Fagherazzi, A Benedetti, S Polizzi, –“A Profile-Fitting Procedure for Analysis of Broadened X-ray Diffraction Peaks: I. Methodology,” J. Appl. Cryst. (1988) 21, 536-542. –“A Profile-Fitting Procedure for Analysis of Broadened X-ray Diffraction Peaks. II. Application and Discussion of the Methodology” J. Appl. Cryst. (1988) 21, 543-549 •B Marinkovic, R de Avillez, A Saavedra, FCR Assunção, “A Comparison between the Warren-Averbach Method and Alternate Methods for X-Ray Diffraction Microstructure Analysis of Polycrystalline Specimens”, Materials Research 4 (2) 71-76, 2001. •D Lou, N Audebrand, “Profile Fitting and Diffraction Line-Broadening Analysis,” Advances in X-ray Diffraction 41, 1997. •A Leineweber, EJ Mittemeijer, “Anisotropic microstrain broadening due to compositional inhomogeneities and its parametrisation”, Z. Kristallogr. Suppl. 23 (2006) 117-122 •BR York, “New X-ray Diffraction Line Profile Function Based on Crystallite Size and Strain Distributions Determined from Mean Field Theory and Statistical Mechanics”, Advances in X-ray Diffraction 41, 1997. What is Microstrain in XRD? What can be calculated from XRD data? How do you calculate lattice parameter from XRD data? How do you calculate micro strain?
